IDENTIFYING DATA 2017_18
Subject (*) ADVANCED SEPARATION PROCESSES Code 20705224
Study programme
Nanoscience, Materials and Processes: Chemical Technology at the Frontier
Cycle 2nd
Descriptors Credits Type Year Period
6 Optional 2Q
Language
Anglès
Department Chemical Engineering
Coordinator
GILABERT ORIOL, GUILLEM
E-mail laureano.jimenez@urv.cat
guillem.gilabert@urv.cat
pezhman.kazemi@urv.cat
bartosz.tylkowski@urv.cat
Lecturers
JIMÉNEZ ESTELLER, LAUREANO
GILABERT ORIOL, GUILLEM
KAZEMI ., PEZHMAN
TYLKOWSKI ., BARTOSZ
Web
General description and relevant information The course deals with modern separation technologies like those listed in contents, for instance: lixiviation, extraction fluidized beds, cristalization and so on. In the second part the course deals with Membrane technology from micro-filtration to ultra- or nano-filtration and reverse osmosis. Finally, there is an introduction to membrane synthesis and microencapsulation.

Competences
Type A Code Competences Specific
 A1.1 A1.1. Successfully studying and learning about the chosen research ambit: evaluating the technical and scientific importance, the technological potential and the viability of the nanoscience, design, preparation, properties, processes, developments, techniques and applications of materials.
 A1.4 A1.4. Conceiving, designing, constructing, reformulating and maintaining equipment, applications and efficient designs for experimental and numerical simulation studies in chemical technology.
Type B Code Competences Transversal
 B1.1 B1.1. Communicating and discussing proposals and conclusions in specialized and non-specialized multilingual forums in a clear and unambiguous manner.
Type C Code Competences Nuclear
 C1.1 Have an intermediate mastery of a foreign language, preferably English

Learning outcomes
Type A Code Learning outcomes
 A1.1 A1.1 Determine the membrane technology to be used according to the characteristics of the species to be separated.
A1.1 Select the right material, structure and configuration of the membrane depending on the properties of the compounds involved.
A1.1 Apply new concepts of operation and sustainable production to the design and process of separation operations.
A1.1 Select the optimal conditions for producing the membrane in accordance with the final application.
A1.1 Select the suitable separation operation given the characteristics of the problem.
A1.1 Design extraction or leaching equipment.
A1.1 Design solid drying processes.
A1.1 Design adsorption, ion exchange or chromatography columns.
A1.1 Design crystallisation equipment.
A1.1 Connect the type of module to the application and membrane material.
A1.1 Establish a suitable rank for the working conditions of each process and separation problem.
A1.1 Design materials for use in the production of membranes with specific properties.
 A1.4 A1.4 Use computer simulation to check the theoretical concepts explained in the classroom.
Type B Code Learning outcomes
 B1.1 B1.1 Can intervene effectively and transmit relevant information.
B1.1 Plan their communication: generate ideas, seek information, select and order information, make schemes, decide on the audience and the aims of the communication, etc.
B1.1 Prepare and deliver structured presentations, complying with the requirements.
B1.1 Draft documents with the appropriate format, content, structure, language accuracy, and register, and can illustrate concepts using the correct conventions: format, headings, footnotes, captions, etc.
B1.1 Use language that is appropriate to the situation.
B1.1 Are aware of the strategies that can be used in oral presentations (audiovisual support, eye contact, voice, gesture, timing, etc.).
Type C Code Learning outcomes
 C1.1 Express opinions on abstract or cultural topics in a limited fashion.
Explain and justify briefly their opinions and projects.
Understand instructions about classes or tasks assigned by the teaching staff.
Understand routine information and articles.
Understand the general meaning of texts that have non-routine information in a familiar subject area.
Write letters or take notes about foreseeable, familiar matters.

Contents
Topic Sub-topic
1. Lixiviation and extraction
2. Solid drying
3. Adsorption, ion exchange and chromatography
4. Crystallisation
5. Membrane technology and microencapsulation (MF, UF, NF, RO, Dialysis, etc). Synthesis of membranes.


Planning
Methodologies  ::  Tests
  Competences (*) Class hours
Hours outside the classroom
(**) Total hours
Introductory activities
2 0 2
Lecture
A1.1
A2.2
A3.1
C1.1
20 39 59
Seminars
A1.1
A1.2
A2.2
A3.1
A3.2
A3.3
B1.1
C1.1
17 30 47
Laboratory practicals
A1.1
A1.2
A2.2
A3.1
A3.2
A3.3
C1.1
13 15 28
Personal tuition
1 0 1
 
Practical tests
A1.1
A1.4
B1.1
C1.1
3 3 6
Oral tests
B1.1
1 1 2
Mixed tests
A1.4
2 2 4
Extended-answer tests
A1.4
B1.1
1 0 1
 
(*) On e-learning, hours of virtual attendance of the teacher.
(**) The information in the planning table is for guidance only and does not take into account the heterogeneity of the students.

Methodologies
Methodologies
  Description
Introductory activities Description of the course and basic definitions
Lecture Expository lectures
Seminars Resolution of exercises or case studies in the classroom
Laboratory practicals Basic laboratory of advanced separation processes: Multipurpose/multiproduct pilot plant, Computer operated distillation pilot plant, membrane laboratory
Personal tuition Meetings outside the classroom, individual or in small groups to discuss on concepts or specific problems. The attention hours will be conveniently informed as well as the communication channels (check Moodle workspace).

Personalized attention
Description
Meetings out of the classroom, at professor office or meeting rooms, on demand via Moodle or email.

Assessment
Methodologies Competences Description Weight        
Practical tests
A1.1
A1.4
B1.1
C1.1
Evaluation of the laboratory work through reports 35%
Oral tests
B1.1
Short exposition over a given topic 15%
Mixed tests
A1.4
Resolution of tests combining short questions and resolution of exercises 35%
Extended-answer tests
A1.4
B1.1
Short tests during the seminar sessions 15%
Others  
 
Other comments and second exam session

In the first call, a minimum mark of 3.5 in each part is demanded to calculate the average. In the second call, the parts not passed will be re-evaluated for those where average cannot be calculated or is lower than 5.0.


Sources of information

Basic Schefflan, Ralph, Teach yourself the basics of Aspen plus, 1st, Wiley-Blackwell
Foo, Dominic, Chemical Engineering Process Simulation, 1st, Elsevier
Puigjaner, Luis; Ollero, Pedro; De Prada, Cesar y Jiménez, ESTRATEGIAS DE MODELADO, SIMULACION Y OPTIMIZACION DE PROCESOS QUIMICOS, 1st, SINTESIS
M. Mulder, Basic Principles of Membrane Technology, 2nd, Kluwer Academic
Luyben, William L., Distillation design and control using Aspen simulation, 1st, John Wiley & Sons
Hanyak, Michael Edward, Chemical process simulation and the Aspen HYSYS software, 1st, Bucknell University

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(*)The teaching guide is the document in which the URV publishes the information about all its courses. It is a public document and cannot be modified. Only in exceptional cases can it be revised by the competent agent or duly revised so that it is in line with current legislation.