IDENTIFYING DATA 2019_20
Subject (*) ADVANCED SEPARATION PROCESSES Code 20705224
Study programme
Nanoscience, Materials and Processes: Chemical Technology at the Frontier
 Cycle 2nd
Descriptors Credits Type Year Period
6 Optional
Language
Anglès
Department Chemical Engineering
Coordinator
JIMÉNEZ ESTELLER, LAUREANO
 E-mail laureano.jimenez@urv.cat
guillem.gilabert@urv.cat
bartosz.tylkowski@urv.cat
fatemeh.rostami@urv.cat
Lecturers
JIMÉNEZ ESTELLER, LAUREANO
GILABERT ORIOL, GUILLEM
TYLKOWSKI , BARTOSZ
ROSTAMI , FATEMEH
Web
General description and relevant information The course deals with modern separation technologies like those listed in contents, for instance: lixiviation, extraction fluidized beds, and so on. In the second part the course deals with Membrane technology from micro-filtration to ultra- or nano-filtration and reverse osmosis. Finally, there is an introduction to membrane synthesis and microencapsulation. On the other hand, we also included advanced modelling strategies for the design, rate and optimization of advance separation strategies in steady state (e.g., petroleum modelling, solid modelling, extractive distillation, reactive distillation, pressure swing separation, azeotropic distillation…) and the fundamental aspects associated with the design of units using dynamic modelling (e.g., CSTR, PFR…). To obtain such results AspenPlus, AspenHysys and/or SuperPro modelling tools are used.

Competences
Type A Code Competences Specific
 A1.1 Effectively apply knowledge of basic, scientific and technological materials pertaining to engineering.
 A1.2 Design, execute and analyze experiments related to engineering.
 A2.2 Conceive, project, calculate and design processes, equipment, industrial installations and services in the field of chemical engineering and related industrial sectors in terms of quality, safety, economics, the rational and efficient use of natural resources and the conservation of the environment. (G2)
 A3.1 Apply knowledge of mathematics, physics, chemistry, biology and other natural sciences by means of study, experience, practice and critical reasoning in order to establish economically viable solutions for technical problems (I1).
 A3.2 Design and optimize products, processes, systems and services for the chemical industry on the basis of various areas of chemical engineering, including processes, transport, separation operations, and chemical, nuclear, elctrochemical and biochemical reactions engineering (I2).
 A3.3 Conceptualize engineering models and apply innovative problems solving methods and appropriate IT applications to the design, simulation, optimization and control of processes and systems (I3).
Type B Code Competences Transversal
 B1.1 Communicate and discuss proposals and conclusions in a clear and unambiguous manner in specialized and non-specialized multilingual forums (G9).
Type C Code Competences Nuclear

Learning outcomes
Type A Code Learning outcomes
 A1.1 Determine the membrane technology to be used according to the characteristics of the species to be separated.
Select the right material, structure and configuration of the membrane depending on the properties of the compounds involved.
 A1.2 Use computer simulation to check the theoretical concepts explained in the classroom.
 A2.2 Apply new concepts of operation and sustainable production to the design and process of separation operations.
Select the optimal conditions for producing the membrane in accordance with the final application.
 A3.1 Select the suitable separation operation given the characteristics of the problem.
 A3.2 Design extraction or leaching equipment.
Design solid drying processes.
Design adsorption, ion exchange or chromatography columns.
Design crystallisation equipment.
Connect the type of module to the application and membrane material.
 A3.3 Establish a suitable rank for the working conditions of each process and separation problem.
Design materials for use in the production of membranes with specific properties.
Type B Code Learning outcomes
 B1.1 Intervene effectively and transmit relevant information.
Prepare and deliver structured presentations that satisfy the stipulated requirements.
Plan the communication: generate ideas, look for information, select and order information, make sketches, identify the audience and the aims of the communication, etc.
Draft documents using the appropriate format, content, structure, language accuracy, and register. Illustrate concepts using the correct conventions: format, headings, footnotes, captions, etc.
Employ the strategies used to make effective oral presentations (audio-visual aids, eye contact, voice, gestures, timing, etc.).
Use language appropriate to the situation.
Produces a grammatically correct oral text
Produce well structured, clear and effective oral texts.
Produce oral texts that are appropriate to the communicative situation.
Produce grammatically correct written texts.
Produce well-structured, clear and rich written texts
Produce written texts that are appropriate to the communicative situation.
Type C Code Learning outcomes

Contents
Topic Sub-topic
1. Lixiviation and extraction
2. Adsorption, ion exchange and chromatography
3. Membrane technology and microencapsulation (MF, UF, NF, RO, Dialysis, etc). Synthesis of membranes.
4. Rigurosos modelling and optimization of advanced separation processes in steady state using AspenPlus and/or AspenHysys and/or SuperPro: petroleum modelling, solid handling (Particle size distribution), extractive distillation, reactive distillation, pressure swing separation, azeotropic distillation…
5. Dynamic modelling of reactive processes using AspenPlus and/or AspenHysys: CSTR, PFR. Tune of control parameters.

Planning
Methodologies  ::  Tests
  Competences (*) Class hours
 Hours outside the classroom
 (**) Total hours
Introductory activities
2 0 2
Lecture
A1.1
A2.2
A3.1
20 39 59
IT-based practicals in computer rooms
A1.1
A1.2
A2.2
A3.1
A3.2
A3.3
B1.1
 13 15 28
Problem solving, exercises
A1.1
A1.2
A2.2
A3.1
A3.2
A3.3
B1.1
 17 30 47
Personal attention
1 0 1
 
Practical tests
A1.1
A1.2
A2.2
A3.1
A3.2
A3.3
B1.1
 3 3 6
Oral tests
A1.1
A1.2
A2.2
A3.1
A3.2
A3.3
B1.1
 1 1 2
Mixed tests
A1.1
A1.2
A2.2
A3.1
A3.2
A3.3
B1.1
 2 2 4
 
(*) On e-learning, hours of virtual attendance of the teacher.
(**) The information in the planning table is for guidance only and does not take into account the heterogeneity of the students.

Methodologies
Methodologies
  Description
Introductory activities Description of the course and basic definitions
Lecture Expository lectures
IT-based practicals in computer rooms Practical application of the theory of a knowledge area in a particular context. Practical exercises using ICTs.
Problem solving, exercises Students analyse and solve problems or practical exercises related to the subject.
Personal attention Meetings outside the classroom, individual or in small groups to discuss on concepts or specific problems. The attention hours will be conveniently informed as well as the communication channels (check Moodle workspace).

Personalized attention
Description
If you want/need any discussion/tutorization, please send me and e-mail (laureano.jimenez@urv.cat), phone me (977558643) or contact me via skype (Laureano Jimenez) so we can schedule a meeting. Office 219 (Chemical Engineering Department). Classes & exam will be in Laboratory 304. Guillem Gilabert: guillem.gilabertoriol@dupont.com or Moodle. Office: 221

Assessment
Methodologies Competences Description Weight        
Problem solving, exercises
A1.1
A1.2
A2.2
A3.1
A3.2
A3.3
B1.1
 Solve individually case studies (2-3). Delivered using moodle. Penalties applicable for late-delivery
 25%
Practical tests
A1.1
A1.2
A2.2
A3.1
A3.2
A3.3
B1.1
 Individual test with a mínimum grade of 4.0/10, in order to pass the course. The máximum grade (MH equivalent to A+) will be obtained based in the individual grades. 25%
Oral tests
A1.1
A1.2
A2.2
A3.1
A3.2
A3.3
B1.1
 Short exposition over a given topic 15%
Mixed tests
A1.1
A1.2
A2.2
A3.1
A3.2
A3.3
B1.1
 Resolution of tests combining short questions and resolution of exercises 35%
Others  
 
Other comments and second exam session

In the first call, a minimum mark of 4 in each part is demanded to calculate the average. In the second call, the parts not passed will be re-evaluated for those where average cannot be calculated or is lower than 5.0.

Sources of information

Basic M. Mulder, Basic Principles of Membrane Technology, 2nd, Kluwer Academic
Foo, Dominic, Chemical Engineering Process Simulation, 1st, Elsevier
Hanyak, Michael Edward, Chemical process simulation and the Aspen HYSYS software, 1st, Bucknell University
Schefflan, Ralph, Teach yourself the basics of Aspen plus, 1st, Wiley-Blackwell
Luyben, William L., Distillation design and control using Aspen simulation, 1st, John Wiley & Sons
Puigjaner, Luis; Ollero, Pedro; De Prada, Cesar y Jiménez, ESTRATEGIAS DE MODELADO, SIMULACION Y OPTIMIZACION DE PROCESOS QUIMICOS, 1st, SINTESIS

Complementary

Recommendations
(*)The teaching guide is the document in which the URV publishes the information about all its courses. It is a public document and cannot be modified. Only in exceptional cases can it be revised by the competent agent or duly revised so that it is in line with current legislation.